The gold ore is first subjected to pre-acidification, with a portion of water added to form a slurry, and appropriate preheating is performed to ensure the temperature conditions in the autoclave. Pressure oxidation (POX) is then carried out in the autoclave at 190°C under an oxygen-rich environment to oxidize pyrite, arsenopyrite, and other sulfides, concurrently releasing the encapsulated gold and generating sulfuric acid and iron arsenate precipitates. The oxidized slurry is sent to a thickener, where the underflow enters countercurrent decantation (CCD) washing to clean the solids, while part of the supernatant is recycled back to pre-acidification and part is neutralized. Finally, a solid oxidized concentrate is obtained, which serves as feedstock for subsequent hydrometallurgical leaching or pyrometallurgical refining.